Presentation
The Institutional Nuclear Magnetic Resonance Laboratory has 6 NMR spectrometers, two of which are for solid state analysis and four for solution analysis, with the possibility of carrying out experiments on different nuclei.
Equipment
Details about the equipment that can be found in the laboratory.

NMR Spectrometer - Bruker Avance III HD 250 MHz
Probe:
• BBO (for solution analysis in 5 mm tube)
Automatic sampler: 16 positions
Sample temperature range: from -20,0 °C to 120,0 °C (BCU I)
Routinely analyzed nuclei: 1H, 13C, 19F, 31P, 15N (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).
• BBO (for solution analysis in 5 mm tube)
Automatic sampler: 16 positions
Sample temperature range: from -20,0 °C to 120,0 °C (BCU I)
Routinely analyzed nuclei: 1H, 13C, 19F, 31P, 15N (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).

NMR Spectrometer - Bruker Avance II+ 300MHz
Probes:
• BB (for solid state analysis in 4mm spinner and maximum rotation of 15 kHz)
• BBI (for solution analysis in 5 mm tube)
Automatic sampler: 16 positions (solution analysis)
Sample temperature range: room temperature (~22 °C)
Routinely analyzed nuclei: 1H, 13C, 15N, 29Si, 31P, 27Al (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).
• BB (for solid state analysis in 4mm spinner and maximum rotation of 15 kHz)
• BBI (for solution analysis in 5 mm tube)
Automatic sampler: 16 positions (solution analysis)
Sample temperature range: room temperature (~22 °C)
Routinely analyzed nuclei: 1H, 13C, 15N, 29Si, 31P, 27Al (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).

NMR Spectrometer - Bruker Avance II+ 400MHz
Probes:
• MAS 4 BL CP BB (for solid state analysis in 4mm spinner and maximum rotation of 15 kHz)
• MAS 4BL CP TRIPLE (for solid state analysis in 4mm spinner and maximum rotation of 15 kHz)
Automatic sampler: no
Sample temperature range: room temperature (~22 °C)
Routinely analyzed nuclei: 1H, 13C, 29Si, 31P, 27Al (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).
• MAS 4 BL CP BB (for solid state analysis in 4mm spinner and maximum rotation of 15 kHz)
• MAS 4BL CP TRIPLE (for solid state analysis in 4mm spinner and maximum rotation of 15 kHz)
Automatic sampler: no
Sample temperature range: room temperature (~22 °C)
Routinely analyzed nuclei: 1H, 13C, 29Si, 31P, 27Al (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).

NMR Spectrometer - Bruker Avance III 400MHz
Probes:
• BBI (for solution analysis in 5 mm tube)
• TBI (for solution analysis in 5 mm tube)
• HR MAS (for semisolid analysis in 4mm spinner and maximum rotation of 15 kHz)
Automatic sampler: 16 positions (solution analysis)
Sample temperature range: from -20,0 °C to 120,0 °C (BCU I)
Routinely analyzed nuclei: 1H, 13C, 15N (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).
• BBI (for solution analysis in 5 mm tube)
• TBI (for solution analysis in 5 mm tube)
• HR MAS (for semisolid analysis in 4mm spinner and maximum rotation of 15 kHz)
Automatic sampler: 16 positions (solution analysis)
Sample temperature range: from -20,0 °C to 120,0 °C (BCU I)
Routinely analyzed nuclei: 1H, 13C, 15N (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).

NMR Spectrometer - Bruker Avance III 500MHz
Probes:
• BBO (for solution analysis in 5 mm tube)
• MIC (for imaging in 10 mm tube)
Automatic sampler: 60 positions (solution analysis)
Sample temperature range: from -80,0 °C to 120,0 °C (BCU II)
Routinely analyzed nuclei: 1H, 13C, 15N, 19F, 11B, 29Si, 31P (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).
• BBO (for solution analysis in 5 mm tube)
• MIC (for imaging in 10 mm tube)
Automatic sampler: 60 positions (solution analysis)
Sample temperature range: from -80,0 °C to 120,0 °C (BCU II)
Routinely analyzed nuclei: 1H, 13C, 15N, 19F, 11B, 29Si, 31P (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).

NMR Spectrometer - Bruker Avance NEO 600MHz
Probes:
Probes for solution analysis in 5 mm tube:
• iProbe SmartProbe TBO BBF
• CryoProbe Prodigy TCI
Automatic sampler: 24 positions
Sample temperature range: from -40,0 °C to 120,0 °C (BCU I)
Routinely analyzed nuclei: 1H, 13C, 15N, 19F, 31P (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).
Probes for solution analysis in 5 mm tube:
• iProbe SmartProbe TBO BBF
• CryoProbe Prodigy TCI
Automatic sampler: 24 positions
Sample temperature range: from -40,0 °C to 120,0 °C (BCU I)
Routinely analyzed nuclei: 1H, 13C, 15N, 19F, 31P (for the analysis of other nuclei, consult the chemists responsible for the NMR Laboratory).

Benchtop NMR Spectrometer – Oxford X-Pulse HFX 60 MHz
Equipped with probes for 5 mm solution NMR tubes and a flow cell.
Capable of analyzing the nuclei ¹H, ¹³C, and ¹⁹F.
Operating temperature: 40 °C (instrument temperature).
Capable of analyzing the nuclei ¹H, ¹³C, and ¹⁹F.
Operating temperature: 40 °C (instrument temperature).
Team

Anderson Santos Pedrosa, B. Sc.

